HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 556388Generated: October 30, 2026
Triethyl phosphite → HCID 12182784, compound
https://huagongshe.com/reaction/556388
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | methyl (2R)-2-(((tert-butoxy)carbonyl)amino)-3-iodopropanoate | HCID 10903591 | — |
| Product | HCID 12182784 | HCID 12182784 | — |
Reaction Steps
Boc-3-iodo-L-Ala-OMe (10 g) was dissolved in triethyl phosphite (79.7 mL). The mixture was heated at 140° C. for 15 h and evaporated to dryness to give the desired compound (9.37 g). It was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08058263B2 |
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| Source dataset | uspto-grants-2011_11 |
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| ORD ID | ord-89ae6921572b4231a6c520ba55ec0433 |
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| Source note | uspto-grants-2011_11 |
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