HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sec-Butylamine → 4-Sec-butylamino-6-chloro-2-methylsulfanyl-pyrimidine-5-carbaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sec-Butylamine | HCID 24874 | — |
| Edukt | 4,6-Dichloro-2-(methylsulfanyl)pyrimidine-5-carbaldehyde | HCID 4614004 | — |
| Produkt | 4-Sec-butylamino-6-chloro-2-methylsulfanyl-pyrimidine-5-carbaldehyde | HCID 59639584 | — |
Reaktionsschritte
Prepared as described above in Example 2 starting from 4,6-dichloro-2-methylsulfanyl-pyrimidine-5-carbaldehyde and 2-butylamine to give the title compound 4-sec-butylamino-6-chloro-2-methylsulfanyl-pyrimidine-5-carbaldehyde. 1H-NMR: δ 0.87 (m, 3H), 1.18 (m, 3H), 1.20 (m, 2H), 2.51 (s, 3H), 4.24 (m, 1H), 9.12 (br s, 1H), 10.18 (s, 1H). LC MS (m/e)=260 (MH+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08058282B2 |
| Quelldatensatz | uspto-grants-2011_11 |
| ORD ID | ord-0bde9e7647ac499891cb149e3e5e4199 |
| Quellennotiz | uspto-grants-2011_11 |