Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Fluorophenylboronic acid → HCID 10132968, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Fluorophenylboronic acid | HCID 2734354 | — |
| 반응물 | 4-Chloro-6-(2-fluoro-phenylamino)-2-methylsulfanyl-pyrimidine-5-carbaldehyde | HCID 9944073 | — |
| 생성물 | HCID 10132968 | HCID 10132968 | — |
반응 단계
Prepared as described above in Example 11 starting from 4-chloro-6-(2-fluoro-phenylamino)-2-methylsulfanyl-pyrimidine-5-carbaldehyde and 2-fluorophenylboronic acid to give the title compound 4-(2-fluoro-phenyl)-6-(2-fluoro-phenylamino)-2-methylsulfanyl-pyrimidine-5-carbaldehyde. 1H-NMR: δ0.61 (s, 3H), 7.11-7.23 (m, 4H), 7.26 (m, 1H), 7.45-7.62 (m, 2H), 8.38 (m, 1H), 9.80 (s, 1H), 11.33 (br s, 1H). LC MS (m/e)=358 (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08058282B2 |
| 출처 데이터셋 | uspto-grants-2011_11 |
| ORD ID | ord-71fe867b7d54419c9d394df497e85184 |
| 출처 메모 | uspto-grants-2011_11 |