HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → HCID 59639572, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | HCID 59639608 | HCID 59639608 | — |
| Product | HCID 59639572 | HCID 59639572 | 48.1% |
Reaction Steps
Following the general procedure outlined in Example 126, the product of Example 121 (200 mg, 0.47 mmol), and cyclohexylamine (0.27 mL, 2.36 mmol) were reacted to give the crude material, which was purified as described in Example 198 to give the desired product 100 mg (48%). LC-MS: 443.4 (MH+, m/z), 2.79 (Rt, min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058282B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-6c70eb76a93945d2a8e7b72054a0834c |
| Source note | uspto-grants-2011_11 |