HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 59639540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | Trimethylaluminum | HCID 16682925 | — |
| Reactant | HCID 59639612 | HCID 59639612 | — |
| Product | HCID 59639540 | HCID 59639540 | — |
Reaction Steps
Following the procedure outlined in Example 193, cyclopropylamine (0.23 mL, 3.3 mmol), trimethylaluminum (1.7 mL, 3.3 mmol) and the product of Example 190 (150 mg, 0.33 mmol) were reacted to give the desired product, 20 mg (13%). LC-MS: 480.0 (MH+, m/z), 1.89 (Rt, min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058282B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-c7c61eaed0e94e5a8ea4fea78e7f5027 |
| Source note | uspto-grants-2011_11 |