HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiomorpholine → HCID 11785794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiomorpholine | HCID 67164 | — |
| Reactant | Trimethylaluminum | HCID 16682925 | — |
| Reactant | HCID 59639612 | HCID 59639612 | — |
| Product | HCID 11785794 | HCID 11785794 | 86.5% |
Reaction Steps
Following the general procedure outlined in Example 193, thiomorpholine (0.22 mL, 2.2 mmol), trimethylaluminum (1.1 mL, 2.2 mmol) and the product of Example 190 (200 mg, 0.44 mmol) were reacted to give the desired product 200 mg (86%). LC-MS: 526.0 (MH+, m/z), 2.07 (Rt, min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058282B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-15f17b7eedc14106a96ca96a39bb2521 |
| Source note | uspto-grants-2011_11 |