HCID 13845546, compound → HCID 66765802, compound

Participants

Reaction Steps

To a solution of 1-deoxy-2,3,4,6-tetra-O-benzyl-1-(2,4-dimethoxyphenyl)-β-D-glucopyranose (1.1 g) in methanol (10 mL) and tetrahydrofuran (5 mL) was added 10% palladium-carbon powder (0.50 g), and the mixture was stirred at room temperature for 5 hours under a hydrogen atmosphere. The insoluble material was removed by filtration, and the solvent of the filtrate was removed under reduced pressure to give the title compound (0.47 g).

Provenance & Evidence