Sodium Methoxide → HCID 66765956, compound

Participants

Reaction Conditions

Reaction Steps

To a suspension of 1-[6-methoxy-3-(2-phenylethyl)-benzo[b]furan-5-yl]-1-deoxy-2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranose (0.03 g) in methanol (4 mL) was added sodium methoxide (28% methanol solution, 0.038 mL), and the mixture was stirred at 50° C. for 6 hours. The reaction mixture was purified directly by column chromatography on silica gel (eluent: dichloromethane/methanol=10/1-5/1) to give the title compound (0.015 g).

Provenance & Evidence