HCID 66765671, compound → HCID 66765806, compound

Participants

Reaction Steps

A solution of 1-[1-(4-methylbenzyl)-1H-indol-6-yl]-1-deoxy-2,3,4,6-tetra-O-benzyl-β-D-glucopyranose and 10% palladium-carbon powder (0.12 g) in tetrahydrofuran (3 mL) and methanol (3 mL) was stirred at room temperature for 1 hour under a hydrogen atmosphere. The insoluble material was removed by filtration, and the filtrate was concentrated under reduced pressure. The residue was purified by column chromatography on silica gel (eluent: dichloromethane/methanol=10/1) to give the title compound (0.035 g).

Provenance & Evidence