HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 2,3-Dimethylbenzo[d]thiazol-3-ium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 2-Methylbenzothiazole | HCID 8446 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2,3-Dimethylbenzo[d]thiazol-3-ium iodide | HCID 459121 | — |
Reaction Steps
14.9 g (12.7 ml, 0.10 mol) 2-methyl-benzothiazole and 28.4 g (12.5 ml, 0.20 mol) iodomethane were boiled for 7 h in 20 ml ethanol. The residue was filtrated and washed with ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058431B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-2f319611653048469c6bea7b7ac85756 |
| Source note | uspto-grants-2011_11 |