Benzenesulfonic Acid → HCID 25070765, compound

Participants

Reaction Steps

3-(3-(4-(Pyridin-2-yloxymethyl)-benzyl)-isoxazol-5-yl)-pyridin-2-yl amine (100 mg) was dissolved in methanol (5 mL) and benzenesulfonic acid (46.3 mg) was added thereto. This solution was stirred at room temperature for 5 minutes, and then, concentrated in vacuo. To the residue was added ethanol (5 mL), and subjected to ultrasound treatment to cause solids to be precipitated. This solids were filtered, washed with ethanol, and then, dried under a reduced pressure to obtain the title compound (107 mg).

Provenance & Evidence