Fumaric Acid → HCID 131729279, compound

Participants

Reaction Conditions

Reaction Steps

3-(3-(4-(Pyridin-2-yloxymethyl)-benzyl)-isoxazol-5-yl)-pyridin-2-yl amine (200 mg) was dissolved in methanol (2.67 mL) and ethyl acetate (2.67 mL), and fumaric acid (64.8 mg) was added thereto. The solvent was concentrated under a reduced pressure, and to the residue was added ethanol (10 mL), and dissolved by heating. Then, the solution was cooled to 0° C to be solidified. The solids were filtered to obtain the title compound (136 mg).

Provenance & Evidence