Succinic Acid → HCID 131729280, compound

Participants

Reaction Steps

3-(3-(4-(Pyridin-2-yloxymethyl)-benzyl)-isoxazol-5-yl)-pyridin-2-yl amine (200 mg) was dissolved in methanol (10 mL), and succinic acid (65.8 mg) was added thereto. This reaction mixture as stirred at room temperature for 5 minutes, and then, concentrated under a reduced pressure. To the residue was added ethanol (10 mL), heated using an oil bath at 60° C, then cooled to 0° C to cause a solid to be precipitated. The solids were collected, washed with ethanol, and then, dried in vacuo to obtain the title compound (83 mg).

Provenance & Evidence