Ether hydrochloride → HCID 86586068, compound

HRID 557311Notes

Reaction equation

HRID 557311 reaction equation
[CH3:1][N:2]1[CH2:7][CH2:6][CH:5]([O:8][C:9]2[CH:14]=[C:13]([CH2:15][NH2:16])[CH:12]=[CH:11][N:10]=2)[CH2:4][CH2:3]1.[ClH:17].CCOCC>CCOCC>[ClH:17].[ClH:17].[CH3:1][N:2]1[CH2:3][CH2:4][CH:5]([O:8][C:9]2[CH:14]=[C:13]([CH2:15][NH2:16])[CH:12]=[CH:11][N:10]=2)[CH2:6][CH2:7]1

Participants

4

Reactant 2

HCID 10953452Ether hydrochlorideHCID 21959563HCID 21959563, compound

Product 1

HCID 86586068HCID 86586068, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

[2-(1-Methylpiperidin-4-yloxy)-pyridin-4-yl]methylamine was diluted with Et2O (50 ml) and 1M HCl/Et2O (47 ml) was added. The vessel was swirled until precipitate formed.

Workup

  1. additionwas added
  2. customformed

Sources & evidence

ORD record
ord-866b6000a066421ebec0fe73aaa94dfe
Source dataset
uspto-grants-2011_11
Patent number
US08058445B2

Reaction notes

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