HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21959544, compound → HCID 21049551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21959544 | HCID 21959544 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21049551 | HCID 21049551 | — |
Reaction Steps
3,3-Dimethyl-1-(1-methyl-piperidin-4-yl)-6-nitro-2,3-dihydro-1H-indole (600 mg, Step E) was dissolved in MeOH (20 mL), the mixture was bubbled with H2 for 10 min. 10% Pd/C (100 mg) was added and the mixture was stirred under H2 overnight. The mixture was filtered through Celite® and concentrated in vacuo to afford the title compound as an oil. MS: 260 (M+1). Calc'd. for C16H25N3−259.39.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08058445B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-ea9c363f5edb4252af7c0657ac2b1624 |
| Source note | uspto-grants-2011_11 |