Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 557364Generated: October 30, 2026

HCID 21959544, compound → HCID 21049551, compound

https://huagongshe.com/reaction/557364

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21959544HCID 21959544—
SolventMethanolHCID 887—
ProductHCID 21049551HCID 21049551—

Reaction Steps

3,3-Dimethyl-1-(1-methyl-piperidin-4-yl)-6-nitro-2,3-dihydro-1H-indole (600 mg, Step E) was dissolved in MeOH (20 mL), the mixture was bubbled with H2 for 10 min. 10% Pd/C (100 mg) was added and the mixture was stirred under H2 overnight. The mixture was filtered through Celite® and concentrated in vacuo to afford the title compound as an oil. MS: 260 (M+1). Calc'd. for C16H25N3−259.39.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08058445B2
Source datasetuspto-grants-2011_11
ORD IDord-ea9c363f5edb4252af7c0657ac2b1624
Source noteuspto-grants-2011_11