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HRID557569

反应详情

EQUATION

反应方程式

HRID 557569 的结构方程式

REACTANTS

反应物

2
结构：II
HCID807

Iodine

I2

结构：COC(=O)c1ccc(N)cc1
HCID12082

Benzoic acid, 4-amino-, methyl ester

C8H9NO2

PRODUCTS

生成物

1
结构：COC(=O)c1ccc2c(c1)C(C)=CC(C)(C)N2
HCID53416110

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)C=C(C)C
溶剂HCID8858

4-Methylpent-3-en-2-one

C6H10O

PROCEDURE

实验过程

Skraup reaction of methyl 4-aminobenzoate (5.0 g) and iodine (1.7 g) in mesityl oxide (25 ml) was performed according to the method described in example 1.