Dimethylformamide → HCID 66662558, compound

Participants

Reaction Steps

A mixture of 4-{1-[(3-pyridin-4-ylpyrrolidin-1-yl)-carbonyl]cyclopropyl}phenol (20 mg, 0.00006 mol, example 372), benzyl bromide (7.7 μL, 0.000065 mol), and potassium carbonate (18 mg, 0.00013 mol) in N,N-dimethylformamide (200 μL, 0.002 mol) was stirred at room temperature over night. The crude product was purified with prep-HPLC to afford the product (10.3 mg). LCMS: m/z 399.0 (M+H+).

Provenance & Evidence