HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → 5-Bromo-N-tert-butylpyridine-3-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | 5-Bromopyridine-3-sulfonyl chloride | HCID 20324474 | — |
| Product | 5-Bromo-N-tert-butylpyridine-3-sulfonamide | HCID 61794951 | 108% |
Reaction Steps
Prepared by general procedure III from 5-bromo-pyridine-3-sulfonyl chloride (Example B.2 step 2) (500 mg, 2 mmol) and tert-butylamine (1.03 mL, 10 mmol) to give the title compound as a white solid (620 mg, 108%). MS (ISP) 293.0 [(M+H)+], 295.2 [(M+2+H)+]. mp 110° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063048B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-c7f1586241b840b6b68175eedb69f9dd |
| Source note | uspto-grants-2011_11 |