HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethanolamine → 5-Bromo-pyridine-3-sulfonic acid bis-(2-hydroxy-ethyl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | 5-Bromopyridine-3-sulfonyl chloride | HCID 20324474 | — |
| Product | 5-Bromo-pyridine-3-sulfonic acid bis-(2-hydroxy-ethyl)-amide | HCID 61797219 | 42% |
Reaction Steps
Prepared by general procedure III from 5-bromo-pyridine-3-sulfonyl chloride (Example B.2 step 2) (500 mg, 2 mmol) and diethanolamine (1.03 g, 10 mmol) to give the title compound as an off-white solid (270 mg, 42%). MS (ISP) 325.1 [(M+H)+], 327.1 [(M+2+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063048B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-c3bdfd57e9e5411db924f000d928fd12 |
| Source note | uspto-grants-2011_11 |