HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → 3-Bromo-N-tert-butylbenzene-1-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Product | 3-Bromo-N-tert-butylbenzene-1-sulfonamide | HCID 4820926 | 106.4% |
Reaction Steps
Prepared by general procedure III from tert-butylamine (3.16 mL, 30 mmol) and commercially available 3-bromobenzenesulfonyl chloride (1.44 mL, 10 mmol) to give the title compound as a light yellow solid (3.11 g, 106%). MS (ISN) 290.1 [(M−H)−], 292.2 [(M+2−H)−].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063048B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-e123073eecd6444fb5e6d4ff93eb615b |
| Source note | uspto-grants-2011_11 |