HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → 5-bromo-2-methylbenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | 5-Bromo-2-methylbenzene-1-sulfonyl chloride | HCID 4962163 | — |
| Product | 5-bromo-2-methylbenzenesulfonamide | HCID 2446821 | 55% |
Reaction Steps
Prepared by general procedure III from 5-Bromo-2-methyl-benzenesulfonyl chloride (1.89 g, 7 mmol) and ammonium hydroxide (20 mL) to give the title compound (0.96 g, 55%) as a white solid. MS (ISN) 248.0 [(M−H)−], 250.0 [(M+2−H)−].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063048B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-c0470a0ce5964e4cb179cac8b3d39ac8 |
| Source note | uspto-grants-2011_11 |