HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → 4-Bromo-N-(2-hydroxyethyl)benzene-1-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | p-Bromobenzenesulfonyl chloride | HCID 7396 | — |
| Product | 4-Bromo-N-(2-hydroxyethyl)benzene-1-sulfonamide | HCID 458569 | 98% |
Reaction Steps
Prepared by general procedure III from 4-bromobenzenesulfonyl chloride (5.0 g, 20 mmol) and ethanolamine (1.32 g, 22 mmol) to give the title compound (5.4 g, 98%) as an off-white solid. MS (ISP) 280.0 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063048B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-0a1b669a655f407db0c46651374c6ab6 |
| Source note | uspto-grants-2011_11 |