HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → 4-((3-Bromophenyl)sulphonyl)morpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Product | 4-((3-Bromophenyl)sulphonyl)morpholine | HCID 3696002 | 98% |
Reaction Steps
Prepared by general procedure III from 3-bromobenzenesulfonyl chloride (5.0 g, 20 mmol) and morpholine (1.89 g, 22 mmol) to give the title compound (5.9 g, 98%) as a white solid. MS (ISP) 306.1 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063048B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-76574043b4e147229c1fbbe5f9eb76d4 |
| Source note | uspto-grants-2011_11 |