HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → 3-Bromo-N-(2-hydroxyethyl)benzene-1-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | m-Bromobenzenesulphonyl chloride | HCID 17943 | — |
| Product | 3-Bromo-N-(2-hydroxyethyl)benzene-1-sulfonamide | HCID 25307187 | 99% |
Reaction Steps
Prepared by general procedure III from 3-bromobenzenesulfonyl chloride (5.0 g, 20 mmol) and ethanolamine (1.32 g, 22 mmol) to give the title compound (5.45 g, 99%) as a white solid. MS (ISP) 280.0 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063048B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-a304ef65e5774d52a9a1f8d1d4abc9b9 |
| Source note | uspto-grants-2011_11 |