HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Iodine chloride → 6-(4-Chloro-phenyl)-3-iodo-8-methyl-imidazo[1,2-a]pyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Iodine chloride | HCID 24640 | — |
| Edukt | 6-(4-Chloro-phenyl)-8-methyl-imidazo[1,2-a]pyridine | HCID 67000262 | — |
| Produkt | 6-(4-Chloro-phenyl)-3-iodo-8-methyl-imidazo[1,2-a]pyridine | HCID 67000648 | 79% |
Reaktionsschritte
Prepared from 6-(4-chloro-phenyl)-8-methyl-imidazo[1,2-a]pyridine (example C.21 step 1) (6.65 g, 27 mmol) and iodine monochloride as described in example C.20 step 3. Obtained the title compound as an off-white solid (8.0 g, 79%). MS (ISP) 369.0 [(M+H)+], 371 [(M+2+H)+].
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08063048B2 |
| Quelldatensatz | uspto-grants-2011_11 |
| ORD ID | ord-5c9461b8604f4478bf063e103cc9c095 |
| Quellennotiz | uspto-grants-2011_11 |