HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromobenzene-1-sulfonamide → HCID 11852514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromobenzene-1-sulfonamide | HCID 2734765 | — |
| Reactant | HCID 86608077 | HCID 86608077 | — |
| Product | HCID 11852514 | HCID 11852514 | — |
Reaction Steps
The title compound was prepared from 3-ethynyl-7-methyl-5-(4-trifluoromethyl-phenyl)-pyrazolo[1,5-a]pyrimidine (example C.12) (75 mg, 0.25 mmol) and 3-bromo-benzenesulfonamide (59 mg, 0.25 mmol) according to general procedure II. Obtained as a yellow solid (48 mg, 42%). MS (ISN) 454.9 [(M−H)−]; mp 214-216° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063048B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-9188b77c5e6c4a8780375543543a195f |
| Source note | uspto-grants-2011_11 |