HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2,4-difluorobenzenesulfonamide → HCID 86608118, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2,4-difluorobenzenesulfonamide | HCID 2773295 | — |
| Reactant | HCID 86608119 | HCID 86608119 | — |
| Product | HCID 86608118 | HCID 86608118 | — |
Reaction Steps
The title compound was prepared from 4-difluoromethyl-8-ethynyl-2-(4-trifluoromethyl-phenyl)-imidazo[1,5-a]pyrimidine (example C.31) (190 mg, 0.56 mmol) and commercially available 5-bromo-2,4-difluoro-benzenesulfonamide (153 mg, 0.56 mmol) according to general procedure II. Obtained as a brown solid (192 mg, 64%). MS (ISN) 527.1 [(M−H)−]; mp 149° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063048B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-d7b3bb440da14087ba796be2fd7618c3 |
| Source note | uspto-grants-2011_11 |