HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 55914Generated: October 29, 2026
p-Toluenesulfonic acid → HCID 131736881, compound
https://huagongshe.com/reaction/55914
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 3,6,7-Trimethyloct-6-en-1-yn-3-ol | HCID 103660 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131736881 | HCID 131736881 | — |
Reaction Steps
650.0 g of 3,6,7-trimethyl-6-octen-1-in-3-ol and 0.63 g of p-toluene sulfonic acid in water are mixed and heated up to a temperature of 40° C. 479.3 g of acetic acid anhydride are added within 2 hours. After ca. 20 hours the reaction mixture is cooled down and distilled to obtain 3,6,7-trimethyl-6-octen-1-in-3-yl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09434676B2 |
|---|
| Source dataset | uspto-grants-2016_09 |
|---|
| ORD ID | ord-9b53bf7513514509b6dd4944d9eab40f |
|---|
| Source note | uspto-grants-2016_09 |
|---|
