HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 2-Phenylhydrazinecarboxaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Phenylhydrazine hydrochloride | HCID 60962 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Methyl formate | HCID 7865 | — |
| Product | 2-Phenylhydrazinecarboxaldehyde | HCID 12154 | 99.8% |
Reaction Steps
25 g of K2CO3 are added to a solution of 20 g of phenylhydrazine hydrochloride in 150 ml of methyl formate and 60 ml of water, and the mixture is refluxed for 1 hour and left at AT for 12 hours with stirring. The precipitate formed is filter-dried, and washed with a propan-2-ol/petroleum ether mixture. 18.8 g of the expected compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063061B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-bac0b619a90d406c8fea04ff37237830 |
| Source note | uspto-grants-2011_11 |