Hydrazine, ethyl-, ethanedioate (1:1) → HCID 66997389, compound

HRID 559149Notes

Reaction equation

HRID 559149 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[C:30](=[O:31])[N:29]([CH3:32])[C:12]2[N:13]([CH3:28])[C:14]3[C:19]([C:11]=2[CH:10]=1)=[CH:18][C:17]([C:20](=O)[C:21]([CH3:26])=[CH:22]N(C)C)=[CH:16][CH:15]=3.C(O)(=O)C(O)=O.[CH2:39]([NH:41][NH2:42])[CH3:40]>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[C:30](=[O:31])[N:29]([CH3:32])[C:12]2[N:13]([CH3:28])[C:14]3[C:19]([C:11]=2[CH:10]=1)=[CH:18][C:17]([C:20]1[N:41]([CH2:39][CH3:40])[N:42]=[CH:22][C:21]=1[CH3:26])=[CH:16][CH:15]=3

Participants

3

Reactant 2

HCID 96181Hydrazine, ethyl-, ethanedioate (1:1)HCID 66997376HCID 66997376, compound

Product 1

HCID 66997389HCID 66997389, compound

Procedure

The process is carried out as indicated in Example 37 above, using 3-(2,4-dichlorophenyl)-6-(3-dimethylamino-2-methylacryloyl)-1,9-dimethyl-1,9-dihydropyrido[2,3-b]indol-2-one from preparation 1.13 above and ethylhydrazine oxalate.

Sources & evidence

ORD record
ord-8cdc7f01dd8141debb905130248014e2
Source dataset
uspto-grants-2011_11
Patent number
US08063061B2

Reaction notes

Loading…