Acetyl chloride → HCID 66998673, compound

HRID 559168Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[C:6]([O:8][CH3:9])[CH:5]=[CH:4][C:3]=1[C:10]1[C:23](=[O:24])[N:22]([CH3:25])[C:13]2[N:14]([CH3:21])[C:15]3[C:20]([C:12]=2[CH:11]=1)=[CH:19][CH:18]=[CH:17][CH:16]=3.[C:26](Cl)(=[O:28])[CH3:27]>>[C:26]([C:18]1[CH:19]=[C:20]2[C:15](=[CH:16][CH:17]=1)[N:14]([CH3:21])[C:13]1[N:22]([CH3:25])[C:23](=[O:24])[C:10]([C:3]3[CH:4]=[CH:5][C:6]([O:8][CH3:9])=[CH:7][C:2]=3[Cl:1])=[CH:11][C:12]2=1)(=[O:28])[CH3:27]

Participants

Reactant 2

HCID 6367Acetyl chloride

HCID 66997594HCID 66997594, compound

Product 1

HCID 66998673HCID 66998673, compound

Procedure

The process is carried out as indicated in Example 60 above, using compound B: 3-(2-chloro-4-methoxyphenyl)-1,9-dimethyl-1,9-dihydropyrido[2,3-b]indol-2-one and acetyl chloride.

Sources & evidence

ORD record: ord-95ca33702b7c4f3f9df52daa7d1ac95d
Source dataset: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08063061B2

Reaction notes

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