Hydrazine, ethyl-, ethanedioate (1:1) → HCID 66997834, compound

HRID 559194Notes

Reaction equation

HRID 559194 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[C:31](=[O:32])[N:30]([CH3:33])[C:12]2[N:13]([CH3:29])[C:14]3[C:19]([C:11]=2[CH:10]=1)=[CH:18][C:17]([C:20](=O)[CH2:21][C:22](=O)[CH2:23][O:24][CH2:25][CH3:26])=[CH:16][CH:15]=3.C(O)(=O)C(O)=O.[CH2:40]([NH:42][NH2:43])[CH3:41]>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[C:31](=[O:32])[N:30]([CH3:33])[C:12]2[N:13]([CH3:29])[C:14]3[C:19]([C:11]=2[CH:10]=1)=[CH:18][C:17]([C:20]1[N:42]([CH2:40][CH3:41])[N:43]=[C:22]([CH2:23][O:24][CH2:25][CH3:26])[CH:21]=1)=[CH:16][CH:15]=3

Participants

3

Reactant 2

HCID 96181Hydrazine, ethyl-, ethanedioate (1:1)HCID 66997991HCID 66997991, compound

Product 1

HCID 66997834HCID 66997834, compound

Procedure

The process is carried out as in Example 37 above, with the compound from Example 80A, 1-[3-(2,4-dichlorophenyl)-1,9-dimethyl-2-oxo-2,9-dihydro-1H-pyrido[2,3-b]indol-6-yl]-4-ethoxybutane-1,3-dione and ethylhydrazine oxalate.

Sources & evidence

ORD record
ord-d2f0e852d2bc47e78f3d14b05bea58d3
Source dataset
uspto-grants-2011_11
Patent number
US08063061B2

Reaction notes

Loading…