Methyl iodide → HCID 66997912, compound

HRID 559204Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[C:29](=[O:30])[N:28]([CH3:31])[C:12]2[N:13]([CH3:27])[C:14]3[C:19]([C:11]=2[CH:10]=1)=[CH:18][C:17]([C:20]1[S:21][CH:22]=[C:23]([CH2:25][OH:26])[N:24]=1)=[CH:16][CH:15]=3.I[CH3:33]>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[C:29](=[O:30])[N:28]([CH3:31])[C:12]2[N:13]([CH3:27])[C:14]3[C:19]([C:11]=2[CH:10]=1)=[CH:18][C:17]([C:20]1[S:21][CH:22]=[C:23]([CH2:25][O:26][CH3:33])[N:24]=1)=[CH:16][CH:15]=3

Participants

Reactant 2

HCID 6328Methyl iodide

HCID 66997921HCID 66997921, compound

Product 1

HCID 66997912HCID 66997912, compound

Procedure

The process is carried out as indicated in Example 101 above, with the compound from Example 95 above, 3-(2,4-dichlorophenyl)-6-(4-hydroxymethylthiazol-2-yl)-1,9-dimethyl-1,9-dihydropyrido[2,3-b]indol-2-one and iodomethane.

Sources & evidence

ORD record: ord-353b05fd1dcd4041a66e9823c73ea682
Source dataset: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08063061B2

Reaction notes

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