tert-Butoxy bis(dimethylamino)methane → HCID 66998183, compound

HRID 559206Notes

Reaction equation

HRID 559206 reaction equation
[C:1]([C:4]1[CH:5]=[C:6]2[C:10](=[CH:11][CH:12]=1)[N:9]([CH3:13])[C:8]1[N:14]([CH3:26])[C:15](=[O:25])[C:16]([C:18]3[CH:23]=[CH:22][C:21]([Cl:24])=[CH:20][CH:19]=3)=[CH:17][C:7]2=1)(=[O:3])[CH3:2].CC(O[CH:32](N(C)C)[N:33]([CH3:35])[CH3:34])(C)C>>[Cl:24][C:21]1[CH:20]=[CH:19][C:18]([C:16]2[C:15](=[O:25])[N:14]([CH3:26])[C:8]3[N:9]([CH3:13])[C:10]4[C:6]([C:7]=3[CH:17]=2)=[CH:5][C:4]([C:1](=[O:3])[CH:2]=[CH:32][N:33]([CH3:35])[CH3:34])=[CH:12][CH:11]=4)=[CH:23][CH:22]=1

Participants

3

Reactant 2

HCID 79885tert-Butoxy bis(dimethylamino)methaneHCID 66998213HCID 66998213, compound

Product 1

HCID 66998183HCID 66998183, compound

Procedure

The process is carried out as indicated in preparation 1.9C above, with compound B 6-acetyl-3-(4-chlorophenyl)-1,9-dimethyl-1,9-dihydropyrido[2,3-b]indol-2-one and Bredereck's reagent.

Sources & evidence

ORD record
ord-0554d7c3fc2a46998c6a1406b2c1f336
Source dataset
uspto-grants-2011_11
Patent number
US08063061B2

Reaction notes

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