Methylhydrazine → 3-(2,4-Dichlorophenyl)-1,9-dimethyl-6-(2-methyl-2H-pyrazol-3-yl)-1,9-dihydropyrido[2,3-b]indol-2-one

HRID 559221Notes

Reaction equation

HRID 559221 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[C:29](=[O:30])[N:28]([CH3:31])[C:12]2[N:13]([CH3:27])[C:14]3[C:19]([C:11]=2[CH:10]=1)=[CH:18][C:17]([C:20](=O)[CH:21]=[CH:22][N:23](C)C)=[CH:16][CH:15]=3.[CH3:32][NH:33]N>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[C:29](=[O:30])[N:28]([CH3:31])[C:12]2[N:13]([CH3:27])[C:14]3[C:19]([C:11]=2[CH:10]=1)=[CH:18][C:17]([C:20]1[N:33]([CH3:32])[N:23]=[CH:22][CH:21]=1)=[CH:16][CH:15]=3

Participants

3

Reactant 2

HCID 6061MethylhydrazineHCID 669973133-(2,4-Dichlorophenyl)-6-(3-dimethylaminoacryloyl)-1,9-dimethyl-1,9-dihydropyrido[2,3-b]indol-2-one

Product 1

HCID 669987993-(2,4-Dichlorophenyl)-1,9-dimethyl-6-(2-methyl-2H-pyrazol-3-yl)-1,9-dihydropyrido[2,3-b]indol-2-one

Procedure

The process is carried out as in Example 37 above, with the compound from preparation 1.10F, 3-(2,4-dichlorophenyl)-6-(3-dimethylaminoacryloyl)-1,9-dimethyl-1,9-dihydropyrido[2,3-b]indol-2-one and methylhydrazine

Sources & evidence

ORD record
ord-03691fb1b6f3444fbc4cc57c2d632e8e
Source dataset
uspto-grants-2011_11
Patent number
US08063061B2

Reaction notes

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