Hydrochloric Acid → HCID 66999410, compound

Participants

Reaction Steps

The above carboxylic acid (27 mg) was suspended in 3 mL of dichloromethane and 0.2 mL of a 4 N solution of HCl in dioxane was added. After 3.5 h, TLC analysis (EtOAc) showed only baseline material thus 5 mL of ether was added and the resulting solid was collected by filtration and dried to yield the title compound (15 mg, 78%); MS, electrospray, 249 (M+H).

Provenance & Evidence