HCID 59197910, compound → HCID 59197930, compound

HRID 560211Notes

Reaction equation

HRID 560211 reaction equation
[N:1]1([C:7]2([C:11]#[N:12])[CH2:10][CH2:9][CH2:8]2)[CH2:6][CH2:5][S:4][CH2:3][CH2:2]1.[C:13]1([Li])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[C:13]1([CH:11]([NH2:12])[C:7]2([N:1]3[CH2:6][CH2:5][S:4][CH2:3][CH2:2]3)[CH2:10][CH2:9][CH2:8]2)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 59197910HCID 59197910, compound2×HCID 178506676HCID 178506676, compound

Product 1

HCID 59197930HCID 59197930, compound

Procedure

The title compound, yellow oil, MS: m/e=263.1 [(M+B)+], was prepared in accordance with the general method of intermediate B from 1-thiomorpholin-4-yl-cyclobutanecarbonitrile (intermediate X) and phenyllithium.

Sources & evidence

ORD record
ord-c712d050eeef40a185dea7dd398c125c
Source dataset
uspto-grants-2011_11
Patent number
US08063098B2

Reaction notes

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