Tolylboronic acid → HCID 58828767, compound

HRID 560330Notes

Reaction equation

Br[C:2]1[S:3][CH:4]=[CH:5][C:6]=1[C:7]([OH:9])=[O:8].B(O)(O)[C:11]1[CH:12]=[CH:13][C:14]([CH3:17])=[CH:15][CH:16]=1>>[C:14]1([CH3:17])[CH:15]=[CH:16][C:11]([C:2]2[S:3][CH:4]=[CH:5][C:6]=2[C:7]([OH:9])=[O:8])=[CH:12][CH:13]=1

Participants

Reactant 2

HCID 79799Tolylboronic acid

HCID 123209712-Bromothiophene-3-carboxylic acid

Product 1

HCID 58828767HCID 58828767, compound

Procedure

prepared by reaction of 2-bromo-thiophene-3-carboxylic acid with p-tolylboronic acid. LC-MS (basic): tR=0.53 min; [M−H]−=217.1.

Sources & evidence

ORD record: ord-c91dcf13e38240028cbc0a6259e1124d
Source dataset: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08063099B2

Reaction notes

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