Tolylboronic acid → 91368-47-7

HRID 560332Notes

Reaction equation

Br[C:2]1[CH:6]=[CH:5][S:4][C:3]=1[C:7]([OH:9])=[O:8].B(O)(O)[C:11]1[CH:12]=[CH:13][C:14]([CH3:17])=[CH:15][CH:16]=1>>[C:14]1([CH3:17])[CH:15]=[CH:16][C:11]([C:2]2[CH:6]=[CH:5][S:4][C:3]=2[C:7]([OH:9])=[O:8])=[CH:12][CH:13]=1

Participants

Reactant 2

HCID 79799Tolylboronic acid

HCID 27396883-Bromothiophene-2-carboxylic acid

Product 1

HCID 496266191368-47-7

Procedure

prepared by reaction of 3-bromo-thiophene-2-carboxylic acid with p-tolylboronic acid. LC-MS (basic): tR=0.50 min; [M−H]−=217.2.

Sources & evidence

ORD record: ord-8df1640873464e7c947a368084e09cdd
Source dataset: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08063099B2

Reaction notes

Loading…