化工社化工社 化学情報印刷レポート · 研究参考用
4-Chlorobenzaldehyde → (4-Chlorophenyl)(4-fluorophenyl)methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chlorobenzaldehyde | HCID 7726 | — |
| 反応物 | 1-Bromo-4-fluorobenzene | HCID 9993 | — |
| 反応物 | alpha-(4-Fluorophenyl)-4-(trifluoromethyl)benzenemethanol | HCID 579773 | — |
| 生成物 | (4-Chlorophenyl)(4-fluorophenyl)methanol | HCID 12634874 | — |
反応手順
The title compound was prepared starting from 6.00 g (34.29 mmol) of 4-bromofluorobenzene and 5.78 g (41.14 mmol) of 4-chlorobenzaldehyde in analogy to the synthesis of the compound from Example 80A. 7.14 g (88% of theory) of the title compound were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08063234B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-7b4bb04677dc490c944a5f29082de05f |
| 出典メモ | uspto-grants-2011_11 |