Hydrochloric Acid → HCID 58392402, compound

Participants

Reaction Steps

A solution of 2.74 g (6.13 mmol) of the compound from Example 44A in 20 ml of tetrahydrofuran was added dropwise to 21.5 ml (21.5 mmol) of a 1N solution of lithium aluminum hydride in tetrahydrofuran in 50 ml of tetrahydrofuran at RT under argon. Stirring at RT for 15 min was followed by addition of 1N hydrochloric acid, extraction with dichloromethane, drying of the organic phase over magnesium sulfate, filtration and concentration. 2.47 g (99% of theory) of the title compound were obtained.

Provenance & Evidence