HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58392215, compound → HCID 58392352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58392215 | HCID 58392215 | — |
| Reactant | HCID 58392342 | HCID 58392342 | — |
| Product | HCID 58392352 | HCID 58392352 | — |
Reaction Steps
The title compound was prepared starting from 85.0 mg (0.24 mmol) of the compound from Example 36 in analogy to the synthesis of the compound from Example 77. Purification by preparative HPLC (RP18 column; mobile phase: acetonitrile-water gradient with addition of 0.1% formic acid) resulted in 86 mg (97% of theory) of the title compound as mixture of diastereomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063234B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-ea23b700c0c54861a0510f185c19b41a |
| Source note | uspto-grants-2011_11 |