HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Bis(2-propoxyethyl)amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Tert-butyl bis(2-propoxyethyl)carbamate | HCID 89410734 | — |
| Product | Bis(2-propoxyethyl)amine | HCID 20405789 | 100% |
Reaction Steps
To a solution of HCl in EtOAc (15 mL, 30 mmol, 2 M) was added tert-butyl bis(2-propoxyethyl)carbamate (1.78 g, 6.15 mmol). The reaction mixture was stirred at rt overnight, then concentrated in vacuo to give the title compound as colorless oil (1.16 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434695B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-90b49a1dfc6343db85c3f460ec35fb42 |
| Source note | uspto-grants-2016_09 |