HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 90022647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | N-(3-bromo-4-(dihexylamino)phenyl)-3-oxobutanamide | HCID 90024279 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 90022647 | HCID 90022647 | 100% |
Reaction Steps
A mixture of N-(3-bromo-4-(dihexylamino)phenyl)-3-oxobutanamide (5.10 g, 11.6 mmol), MeOH (60 mL) and ammonia (60 mL) was stirred at rt overnight. The mixture was then concentrated in vacuo to give the title compound as black oil (5.10 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434695B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-f358ffae61e542a384a93953d19b0ebe |
| Source note | uspto-grants-2016_09 |