HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Methanesulfonylethyl)(methyl)amine → HCID 16037910, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Methanesulfonylethyl)(methyl)amine | HCID 3856040 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | 3-[1-(ethylsulfonyl)-4-piperidinyl]-5-(3-formylphenyl)-1H-indole-7-carboxamide | HCID 57732804 | — |
| Product | HCID 16037910 | HCID 16037910 | 31% |
Reaction Steps
Following the general procedure of example 1, 3-[1-(ethylsulfonyl)-4-piperidinyl]-5-(3-formylphenyl)-1H-indole-7-carboxamide (42.0 mg, 0.096 mmol), N-methyl-2-(methylsulfonyl)ethanamine (12.0 mg, 0.087 mmol) and NaBH(OAc)3 (58.0 mg, 0.261 mmol) were reacted to give the title compound (15.1 mg, 28.0%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063071B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-f7f5f83770c24e4bbc8cb39239d511ea |
| Source note | uspto-grants-2011_11 |