HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bis(2-Methoxyethyl)amine → HCID 16038008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bis(2-Methoxyethyl)amine | HCID 2383 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | 3-[1-(ethylsulfonyl)-4-piperidinyl]-5-(3-formylphenyl)-1H-indole-7-carboxamide | HCID 57732804 | — |
| Product | HCID 16038008 | HCID 16038008 | 16.8% |
Reaction Steps
Following the general procedure of example 1, 3-[1-(ethylsulfonyl)-4-piperidinyl]-5-(3-formylphenyl)-1H-indole-7-carboxamide (50.0 mg, 0.112 mmol), 2-(methyloxy)-N-[2-(methyloxy)ethyl]ethanamine (114.3 mg, 0.86 mmol) and NaBH(OAc)3 (58.0 mg, 0.303 mmol) were reacted to give the title compound (10.5 mg, 16%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063071B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-b603ea82391b46139894971715bd9e55 |
| Source note | uspto-grants-2011_11 |