HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylethylamine → HCID 66723259, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylethylamine | HCID 12219 | — |
| Reactant | HCID 66723263 | HCID 66723263 | — |
| Product | HCID 66723259 | HCID 66723259 | 44.5% |
Reaction Steps
The title compound was prepared according to the general procedure of 5-(5-{[ethyl(methyl)amino]methyl}-3-thienyl)-3-[1-(ethylsulfonyl)-4-piperidinyl]-1H-indole-7-carboxamide trifluoroacetate, substituting N,N-diethyl-N′-methyl-1,2-ethanediamine (130 mg, 1.0 mmol) for N-methylethanamine to afford 30.0 mg of the title compound (44.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063071B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-8e3fcfb734f24f6e89230b50c7c49222 |
| Source note | uspto-grants-2011_11 |