HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 66722810, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | N,N-Diethylethylenediamine | HCID 60993 | — |
| Reactant | HCID 66723089 | HCID 66723089 | — |
| Product | HCID 66722810 | HCID 66722810 | 42% |
Reaction Steps
The title compound was prepared according to the general procedure of 3-[1-(ethylsulfonyl)-4-piperidinyl]-5-(1-{2-[(2-hydroxyethyl)amino]ethyl}-1H-pyrazol-4-yl)-1H-indole-7-carboxamide trifluoroacetate, substituting N,N-diethyl-1,2-ethanediamine (50 mg, 0.43 mmol) for the 2-aminoethanol to afford 12 mg of the title compound (42%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063071B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-add0c156898f481191786d8aa0f278a1 |
| Source note | uspto-grants-2011_11 |