HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 66722816, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 66723061 | HCID 66723061 | — |
| Product | HCID 66722816 | HCID 66722816 | 16% |
Reaction Steps
The title compound was prepared according to the general procedure of 5-[3-[(dimethylamino)methyl]-4-(methyloxy)phenyl]-3-[1-(ethylsulfonyl)-4-piperidinyl]-1H-indole-7-carboxamide trifluoroacetate, substituting methylamine (50 μL, 0.214 mmol) for the dimethylamine to afford 10 mg of the title compound (16%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08063071B2 |
| Source dataset | uspto-grants-2011_11 |
| ORD ID | ord-6e5e1af6d9ec4471b527358028d8b567 |
| Source note | uspto-grants-2011_11 |