3,4-Dimethylphenol → 1,2-Dimethyl-4-[(prop-2-yn-1-yl)oxy]benzene

HRID 562656Notes

Reaction equation

[CH3:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[CH:6][C:7]=1[CH3:8].[CH2:10](O)[C:11]#[CH:12]>>[CH3:1][C:2]1[CH:3]=[C:4]([O:9][CH2:12][C:11]#[CH:10])[CH:5]=[CH:6][C:7]=1[CH3:8]

Participants

Reactant 2

HCID 72493,4-Dimethylphenol

HCID 7859Propargyl alcohol

Product 1

HCID 134070711,2-Dimethyl-4-[(prop-2-yn-1-yl)oxy]benzene

Procedure

The title compound was synthesized using 3,4-dimethylphenol and propargyl alcohol by conducting a reaction similar to that mentioned in Reference example 35.

Workup

customa reaction similar to

Sources & evidence

ORD record: ord-e00110a77c4746719dd29780e2fd76ab
Source dataset: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08067396B2

Reaction notes

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